From f1ba27a9a5c2e958c5422ecf957172aa79b8c5a3 Mon Sep 17 00:00:00 2001 From: kevcruse96 Date: Thu, 24 Mar 2022 16:46:27 -0700 Subject: [PATCH] Update annotated corpus (2022-03-24) --- data/synthesis_action_annotated_dataset_2021-10-17.json | 1 - data/synthesis_action_annotated_dataset_2022-03-24.json | 1 + 2 files changed, 1 insertion(+), 1 deletion(-) delete mode 100644 data/synthesis_action_annotated_dataset_2021-10-17.json create mode 100644 data/synthesis_action_annotated_dataset_2022-03-24.json diff --git a/data/synthesis_action_annotated_dataset_2021-10-17.json b/data/synthesis_action_annotated_dataset_2021-10-17.json deleted file mode 100644 index 40ad7e7..0000000 --- a/data/synthesis_action_annotated_dataset_2021-10-17.json +++ /dev/null @@ -1 +0,0 @@ -[{"sentence": "Then , both solutions were injected simultaneously drop by drop into hot solution .", "annotations": [{"token": "Then", "tag": ""}, {"token": ",", "tag": ""}, {"token": "both", "tag": ""}, {"token": "solutions", 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{"sentence": "SBA-15 was prepared according to a well established procedure reported by Zhao et. al. 4 g of Pluronic P123 ( Aldrich ) was dissolved in 125 g of 2 M HCl at 35 \u00b0 C with stirring .", "annotations": [{"token": "SBA-15", "tag": ""}, {"token": "was", "tag": ""}, {"token": "prepared", "tag": "Starting"}, {"token": "according", "tag": ""}, {"token": "to", "tag": ""}, {"token": "a", "tag": ""}, {"token": "well", "tag": ""}, {"token": "established", "tag": ""}, {"token": "procedure", "tag": ""}, {"token": "reported", "tag": ""}, {"token": "by", "tag": ""}, {"token": "Zhao", "tag": ""}, {"token": "et.", "tag": ""}, {"token": "al.", "tag": ""}, {"token": "4", "tag": ""}, {"token": "g", "tag": ""}, {"token": "of", "tag": ""}, {"token": "Pluronic", "tag": ""}, {"token": "P123", "tag": ""}, {"token": "(", "tag": ""}, {"token": "Aldrich", "tag": ""}, {"token": ")", "tag": ""}, {"token": "was", "tag": ""}, {"token": "dissolved", "tag": "Mixing"}, {"token": "in", "tag": ""}, 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"using", "tag": ""}, {"token": "NH3\u00b7H2O", "tag": ""}, {"token": ".", "tag": ""}]}, {"sentence": "The resulting suspension was poured with isopropanol and zirconia balls in a bottle which was placed in a \" turbula \" for 24 h at 100 rpm .", "annotations": [{"token": "The", "tag": ""}, {"token": "resulting", "tag": ""}, {"token": "suspension", "tag": ""}, {"token": "was", "tag": ""}, {"token": "poured", "tag": "Miscellaneous"}, {"token": "with", "tag": ""}, {"token": "isopropanol", "tag": ""}, {"token": "and", "tag": ""}, {"token": "zirconia", "tag": ""}, {"token": "balls", "tag": ""}, {"token": "in", "tag": ""}, {"token": "a", "tag": ""}, {"token": "bottle", "tag": ""}, {"token": "which", "tag": ""}, {"token": "was", "tag": ""}, {"token": "placed", "tag": ""}, {"token": "in", "tag": ""}, {"token": "a", "tag": ""}, {"token": "\"", "tag": ""}, {"token": "turbula", "tag": ""}, {"token": "\"", "tag": ""}, {"token": "for", "tag": ""}, {"token": "24", "tag": ""}, {"token": "h", "tag": 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to remove water content from the slurry .", "annotations": [{"token": "The", "tag": ""}, {"token": "wet", "tag": ""}, {"token": "brown", "tag": ""}, {"token": "coloured", "tag": ""}, {"token": "slurry", "tag": ""}, {"token": "was", "tag": ""}, {"token": "subjected", "tag": ""}, {"token": "to", "tag": ""}, {"token": "heat", "tag": "Heating"}, {"token": "treatment", "tag": "Heating"}, {"token": "in", "tag": ""}, {"token": "oven", "tag": ""}, {"token": "at", "tag": ""}, {"token": "100", "tag": ""}, {"token": "\u00b0", "tag": ""}, {"token": "C", "tag": ""}, {"token": "for", "tag": ""}, {"token": "12", "tag": ""}, {"token": "h", "tag": ""}, {"token": "to", "tag": ""}, {"token": "remove", "tag": ""}, {"token": "water", "tag": ""}, {"token": "content", "tag": ""}, {"token": "from", "tag": ""}, {"token": "the", "tag": ""}, {"token": "slurry", "tag": ""}, {"token": ".", "tag": ""}]}, {"sentence": "Ce0.8Sm0.2O1.9 ( SDC ) powders were prepared by EDTA - citric complexing method which was as the 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ceramic specimens were prepared by solid - state reaction of BaCO3 and In2O3 .", "annotations": [{"token": "Ba2In2O5", "tag": ""}, {"token": "ceramic", "tag": ""}, {"token": "specimens", "tag": ""}, {"token": "were", "tag": ""}, {"token": "prepared", "tag": "Starting"}, {"token": "by", "tag": ""}, {"token": "solid", "tag": ""}, {"token": "-", "tag": ""}, {"token": "state", "tag": ""}, {"token": "reaction", "tag": ""}, {"token": "of", "tag": ""}, {"token": "BaCO3", "tag": ""}, {"token": "and", "tag": ""}, {"token": "In2O3", "tag": ""}, {"token": ".", "tag": ""}]}, {"sentence": "Magnetite ( Fe3O4 ) nanoparticles were prepared in a chemical co-precipitation step of ferric and ferrous ions in an alkaline solution .", "annotations": [{"token": "Magnetite", "tag": ""}, {"token": "(", "tag": ""}, {"token": "Fe3O4", "tag": ""}, {"token": ")", "tag": ""}, {"token": "nanoparticles", "tag": ""}, {"token": "were", "tag": ""}, {"token": "prepared", "tag": "Starting"}, {"token": "in", "tag": ""}, 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treatment of FeOOH at 450 \u00b0 C led to the formation of ferric oxide ( Fe2O3 ) .", "annotations": [{"token": "Thermal", "tag": "Heating"}, {"token": "treatment", "tag": "Heating"}, {"token": "of", "tag": ""}, {"token": "FeOOH", "tag": ""}, {"token": "at", "tag": ""}, {"token": "450", "tag": ""}, {"token": "\u00b0", "tag": ""}, {"token": "C", "tag": ""}, {"token": "led", "tag": ""}, {"token": "to", "tag": ""}, {"token": "the", "tag": ""}, {"token": "formation", "tag": ""}, {"token": "of", "tag": ""}, {"token": "ferric", "tag": ""}, {"token": "oxide", "tag": ""}, {"token": "(", "tag": ""}, {"token": "Fe2O3", "tag": ""}, {"token": ")", "tag": ""}, {"token": ".", "tag": ""}]}, {"sentence": "After the autoclave was cooled to room temperature , the precipitates were collected , washed with DI water and acetone , and dried in air .", "annotations": [{"token": "After", "tag": ""}, {"token": "the", "tag": ""}, {"token": "autoclave", "tag": ""}, {"token": "was", "tag": ""}, {"token": 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Sb2O3 ( Sigma Aldrich ) was deposited onto TiO2 ( Kronos , anatase modification ) and stirred for 1 h followed by adding 25 % ammonia solution drop - wisely to adjust pH 7 .", "annotations": [{"token": "In", "tag": ""}, {"token": "the", "tag": ""}, {"token": "first", "tag": ""}, {"token": "step", "tag": ""}, {"token": ",", "tag": ""}, {"token": "Sb2O3", "tag": ""}, {"token": "(", "tag": ""}, {"token": "Sigma", "tag": ""}, {"token": "Aldrich", "tag": ""}, {"token": ")", "tag": ""}, {"token": "was", "tag": ""}, {"token": "deposited", "tag": "Mixing"}, {"token": "onto", "tag": ""}, {"token": "TiO2", "tag": ""}, {"token": "(", "tag": ""}, {"token": "Kronos", "tag": ""}, {"token": ",", "tag": ""}, {"token": "anatase", "tag": ""}, {"token": "modification", "tag": ""}, {"token": ")", "tag": ""}, {"token": "and", "tag": ""}, {"token": "stirred", "tag": "Mixing"}, {"token": "for", "tag": ""}, {"token": "1", "tag": ""}, {"token": "h", "tag": ""}, {"token": "followed", "tag": ""}, {"token": "by", 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99.0 % ) , La2O3 ( 99.95 % ) and TiO2 ( 98.0 % ) with molar ratio Pb : La : Ti = 1.05 : 0.1 : 0.975 were mixed .", "annotations": [{"token": "The", "tag": ""}, {"token": "PbO", "tag": ""}, {"token": "(", "tag": ""}, {"token": "99.0", "tag": ""}, {"token": "%", "tag": ""}, {"token": ")", "tag": ""}, {"token": ",", "tag": ""}, {"token": "La2O3", "tag": ""}, {"token": "(", "tag": ""}, {"token": "99.95", "tag": ""}, {"token": "%", "tag": ""}, {"token": ")", "tag": ""}, {"token": "and", "tag": ""}, {"token": "TiO2", "tag": ""}, {"token": "(", "tag": ""}, {"token": "98.0", "tag": ""}, {"token": "%", "tag": ""}, {"token": ")", "tag": ""}, {"token": "with", "tag": ""}, {"token": "molar", "tag": ""}, {"token": "ratio", "tag": ""}, {"token": "Pb", "tag": ""}, {"token": ":", "tag": ""}, {"token": "La", "tag": ""}, {"token": ":", "tag": ""}, {"token": "Ti", "tag": ""}, {"token": "=", "tag": ""}, {"token": "1.05", "tag": ""}, {"token": ":", "tag": ""}, {"token": "0.1", "tag": ""}, {"token": ":", 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\u00b0 C in air and then ground after cooling .", "annotations": [{"token": "The", "tag": ""}, {"token": "precursor", "tag": ""}, {"token": "was", "tag": ""}, {"token": "initially", "tag": ""}, {"token": "decomposed", "tag": "Heating"}, {"token": "at", "tag": ""}, {"token": "400", "tag": ""}, {"token": "\u00b0", "tag": ""}, {"token": "C", "tag": ""}, {"token": "in", "tag": ""}, {"token": "air", "tag": ""}, {"token": "and", "tag": ""}, {"token": "then", "tag": ""}, {"token": "ground", "tag": "Mixing"}, {"token": "after", "tag": ""}, {"token": "cooling", "tag": "Cooling"}, {"token": ".", "tag": ""}], "remark": "Sol-Gel", "doi": "10.1016/S0378-7753(03)00155-1"}, {"sentence": "The resultant products were collected by filtration and washed sequentially with ethanol and deionized water several times .", "annotations": [{"token": "The", "tag": ""}, {"token": "resultant", "tag": ""}, {"token": "products", "tag": ""}, {"token": "were", "tag": ""}, {"token": "collected", "tag": "Purification"}, 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prepared by a two - step NaAl5O8-LiAl5O8 reaction synthesis procedure as described in Li et al.[ ] Precursor NaAl5O8 was first synthesized from a sol - gel method .", "annotations": [{"token": "Synthesis", "tag": ""}, {"token": "of", "tag": ""}, {"token": "Battery", "tag": ""}, {"token": "Materials", "tag": ""}, {"token": ":", "tag": ""}, {"token": "The", "tag": ""}, {"token": "Na-\u03b2''-Al2O3", "tag": ""}, {"token": "electrolyte", "tag": ""}, {"token": "was", "tag": ""}, {"token": "prepared", "tag": "Starting"}, {"token": "by", "tag": ""}, {"token": "a", "tag": ""}, {"token": "two", "tag": ""}, {"token": "-", "tag": ""}, {"token": "step", "tag": ""}, {"token": "NaAl5O8-LiAl5O8", "tag": ""}, {"token": "reaction", "tag": ""}, {"token": "synthesis", "tag": ""}, {"token": "procedure", "tag": ""}, {"token": "as", "tag": ""}, {"token": "described", "tag": ""}, {"token": "in", "tag": ""}, {"token": "Li", "tag": ""}, {"token": "et", "tag": ""}, {"token": "al.[", "tag": ""}, {"token": "]", 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{"sentence": "The polycrystalline samples of the series Y[Fe1\u2212 xCox(CN)6]\u00b7nH2O were prepared by the co-precipitation method , mixing aqueous solutions of equimolar amounts of K3[Fe(CN)6] , K3[Co(CN)6] and Y(NO3)3\u00b76H2O under continuous stirring at 60 \u00b0 C for 2 h .", "annotations": [{"token": "The", "tag": ""}, {"token": "polycrystalline", "tag": ""}, {"token": "samples", "tag": ""}, {"token": "of", "tag": ""}, {"token": "the", "tag": ""}, {"token": "series", "tag": ""}, {"token": "Y[Fe1\u2212", "tag": ""}, {"token": "xCox(CN)6]\u00b7nH2O", "tag": ""}, {"token": "were", "tag": ""}, {"token": "prepared", "tag": "Starting"}, {"token": "by", "tag": ""}, {"token": "the", "tag": ""}, {"token": "co-precipitation", "tag": ""}, {"token": "method", "tag": ""}, {"token": ",", "tag": ""}, {"token": "mixing", "tag": "Mixing"}, {"token": "aqueous", "tag": ""}, {"token": "solutions", "tag": ""}, {"token": "of", "tag": ""}, {"token": "equimolar", "tag": ""}, {"token": "amounts", 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needles of Bi6ZnO7(AsO4)2 were found in polyphasic melts obtained after heating the mixture 0.5Bi2O3 + ZnO + 0.5As2O5 at 950 \u00b0 C ( respectively 0.25 g of Bi2O3 , 0.05 g of K2CO3 and 0.1 g of As2O5 ) in opened gold tube followed by a slow cooling ramp ( 3 \u00b0 C h\u22121 ) until 600 \u00b0 C .", "annotations": [{"token": "The", "tag": ""}, {"token": "transparent", "tag": ""}, {"token": "colorless", "tag": ""}, {"token": "needles", "tag": ""}, {"token": "of", "tag": ""}, {"token": "Bi6ZnO7(AsO4)2", "tag": ""}, {"token": "were", "tag": ""}, {"token": "found", "tag": ""}, {"token": "in", "tag": ""}, {"token": "polyphasic", "tag": ""}, {"token": "melts", "tag": ""}, {"token": "obtained", "tag": "Starting"}, {"token": "after", "tag": ""}, {"token": "heating", "tag": "Heating"}, {"token": "the", "tag": ""}, {"token": "mixture", "tag": ""}, {"token": "0.5Bi2O3", "tag": ""}, {"token": "+", "tag": ""}, {"token": "ZnO", "tag": ""}, {"token": "+", "tag": ""}, {"token": "0.5As2O5", "tag": 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using a sol - gel method .", "annotations": [{"token": "The", "tag": ""}, {"token": "CuO", "tag": ""}, {"token": "-", "tag": ""}, {"token": "CrOx", "tag": ""}, {"token": "composite", "tag": ""}, {"token": "oxide", "tag": ""}, {"token": "support", "tag": ""}, {"token": "was", "tag": ""}, {"token": "prepared", "tag": "Starting"}, {"token": "using", "tag": ""}, {"token": "a", "tag": ""}, {"token": "sol", "tag": ""}, {"token": "-", "tag": ""}, {"token": "gel", "tag": ""}, {"token": "method", "tag": ""}, {"token": ".", "tag": ""}], "remark": "Sol-Gel", "doi": "10.1016/j.apsusc.2018.02.099"}, {"sentence": "The resulting mixture was then sealed and stirred for 12 h at 110 \u00b0 C .", "annotations": [{"token": "The", "tag": ""}, {"token": "resulting", "tag": ""}, {"token": "mixture", "tag": ""}, {"token": "was", "tag": ""}, {"token": "then", "tag": ""}, {"token": "sealed", "tag": "Non-altering"}, {"token": "and", "tag": ""}, {"token": "stirred", "tag": "Mixing"}, {"token": "for", "tag": ""}, 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aqueous 0.9 % NaCl .", "annotations": [{"token": "After", "tag": ""}, {"token": "5", "tag": ""}, {"token": "min", "tag": ""}, {"token": ",", "tag": ""}, {"token": "2", "tag": ""}, {"token": "\u03bcl", "tag": ""}, {"token": "isobutylchloroformate", "tag": ""}, {"token": "was", "tag": ""}, {"token": "added", "tag": "Mixing"}, {"token": ",", "tag": ""}, {"token": "and", "tag": ""}, {"token": "the", "tag": ""}, {"token": "solution", "tag": ""}, {"token": "was", "tag": ""}, {"token": "left", "tag": "Reaction"}, {"token": "for", "tag": ""}, {"token": "30", "tag": ""}, {"token": "min", "tag": ""}, {"token": "at", "tag": ""}, {"token": "4", "tag": ""}, {"token": "\u00b0", "tag": ""}, {"token": "C", "tag": ""}, {"token": "before", "tag": ""}, {"token": "being", "tag": ""}, {"token": "added", "tag": "Mixing"}, {"token": "to", "tag": ""}, {"token": "4.5", "tag": ""}, {"token": "mg", "tag": ""}, {"token": "(", "tag": ""}, {"token": "2.5", "tag": ""}, {"token": "\u03bcmol", "tag": ""}, {"token": 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