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biochem_fan edited this page Jun 4, 2024
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Welcome to the MicroED wiki!
Data collection, transfer and processing scripts and documentations are in our repository.
- Talos Arctica (200 kV)
- Ceta or Falcon3
- Automated data collection with SerialEM
以下のどちらかの窓口から相談・申請してください。
従来の X 線結晶回折法では解けない試料(1 um 以下のナノ結晶や混合物)を優先しています。結晶が十分に大きいと判断した時は、放射光 X 線を紹介することがあります。また、試料の性状や実験目的によっては、HRTEM や STEM など実空間でのイメージングを推奨することがあります(我々の装置では不可能)。
We prioritize samples that are not amenable to X-ray crystallography, e.g. nano-crystals smaller than 1 um and/or mixtures. When the sample turns out to be large enough, we might refer it to synchrotron X-ray beamlines. Depending on the sample and the goal of the experiment, we might recommend real-space methods such as HRTEM and STEM at other facilities.
- 中根 崇智, 「MicroED：どんな試料に適しているか」 Peptide Newsletter Japan 解説記事, 2023
- 中根 崇智, "High multiplicity MicroED with high-throughput measurements", 第 2 回アグロデザイン学術セミナー 基調講演, 2022 年 12 月 26 日 講演ビデオ
- Sasaki, Nakane et al. "Microcrystal Electron Diffraction (MicroED) Structure Determination of a Mechanochemically Synthesized Co-crystal not Affordable from Solution Crystallization", CrystEngComm, 2023
- Gogoi, Sasaki et al. "Structure elucidation of olanzapine molecular salts by combining mechanochemistry and MicroED", Cryst. Growth Des., 2023
- Aijima, Ueda et al. "Versatile Biaryls and Fused Aromatics through Oxidative Coupling of Hydroquinones with (Hetero)Arenes", ChemistrySelect, 2024
- Sasaki, Nakane et al. "Mechanically-Sensitive Fluorochromism by Molecular Domino Transformation in a Schiff Base Crystal", J. Mater. Chem. C, 2024
From our Talos Arctica/Ceta:
- XRD-00251 (MicroED dataset of a tricyclic bromine compound)
- XRD-00250 (MicroED dataset of a Ni complex)
- XRD-00176 (MicroED dataset of Na2SiF6)
- XRD-00142 (MicroED dataset of pigment crystals that show domino transformation)
- XRD-00126 (MicroED datasets of olanzapinium succinate and two impurities)
- XRD-00125 (MicroED dataset of olanzapinium oxalate)
- XRD-00124 (MicroED dataset of clathrate-II ice (?) and hexagonal ice)
- XRD-00109 (MicroED dataset of solid-state synthesized 2:1 co-crystals of 2-aminopyridine and succinic acid)
- XRD-00103 (MicroED dataset of Biotin)
- XRD-00102 (MicroED dataset of Histidine)
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XRD-00101 (MicroED dataset of Sodium Glutamate Monohydrate (Ajinomoto))
See also a companion dataset by X-ray: XRD-00094 (Sodium Glutamate Monohydrate ("Ajinomoto") from a Rigaku HyPix 6000 detector) - XRD-00100 (MicroED dataset of Sucrose)
- XRD-00099 (MicroED dataset of Ribitol)
- XRD-00098 (MicroED dataset of Trehalose)
From other scopes (data processing collaboration/consultation):
- XRD-00178 (MicroED dataset of tetracycline collected on a Falcon3 detector) from University of Tokyo
- XRD-00177 (MicroED dataset of biotin collected on a Falcon 3 detector) from University of Tokyo
- XRD-00162 (MicroED dataset of thienothienobenzofurane (Compound 6)) from FBS, UOsaka
- XRD-00150 (MicroED dataset of nifedipine collected on CRYO ARM 300 II and TVIPS XF416) from Kyushu University
- XRD-00149 (MicroED dataset of dexamethasone collected on CRYO ARM 300 II and TVIPS XF416) from Kyushu University
- XRD-00141 (MicroED dataset of histidine collected with Direct Electron Apollo) from JEOL
- XRD-00140 (MicroED dataset of sodium glutamate collected with Direct Electron Apollo) from JEOL
- XRD-00139 (MicroED dataset of sucrose collected on CRYO ARM 200 II/Gatan Rio) from Tsukuba University
- XRD-00138 (MicroED dataset of sodium glutamate collected on CRYO ARM 200 II/Gatan Rio) from Tsukuba University
- XRD-00137 (MicroED dataset of hemin collected with EPU-D) from KEK-SBRC
- XRD-00136 (MicroED dataset of sodium glutamate collected with EPU-D) from KEK-SBRC
- XRD-00135 (MicroED dataset of biotin collected with EPU-D) from KEK-SBRC